Barbara GIROUD
Engineer
Contact
barbara.giroud[@]isa-lyon.fr
Research
Quantification of targeted contaminants (pesticides, drugs, plastic additives …) at trace level in complex environmental and biological matrices (honey bees, water, sediments, blood, organs …). Specialized in sample preparation (SPE, QuEChERS, μSLE, ASE …) and quantification method development by LC-MS / MS.
Biography
Barbara Giroud graduated with a DUT in Chemical Engineering in 1995 (University of Lyon 1). In 1999, she joined the CNRS central analysis service at Solaize (69) in the electrochemistry service.
In 2004, she joined the mass spectrometry team. She is trained on the different mass spectrometers coupled with liquid chromatography of the team to quantifie impurity in complex matrices (LC-MS/MS) and to measure the exact mass of organic compounds (ToF).
Since 2010, she has been working in the TRACES research team where she is a specialist in targeted method development by LC-MS / MS in the field of environment and health. She develops innovative analytical methods to quantify trace and ultra-trace contaminants of priority or emerging contaminants and is responsible for dedicated analysis equipment. She joined the UMR 5280 in 2012. For more than ten years, she has been involved in the problem of excess mortality of bees and is a specialist in bee matrices analyzes. Very concerned about safety, she is a workplace first-aid representative and a member of the health and safety commission since its creation at ISA.
Keywords
LC-MS/MS, sample preparation, method development, target analysis, quantification, traces analysis, environment, health
Publications
2022
Journal articles
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- Paul Rocchi, Lucie Labied, Tristan Doussineau, Michel Julien, Barbara Giroud, et al.. Identification of Molecular Fragments in Equilibrium with Polysiloxane Ultrasmall Nanoparticles. Nanomaterials, 2022, 12 (5), pp.738. ⟨10.3390/nano12050738⟩. ⟨hal-03940522⟩
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- Paul Rocchi, Lucie Labied, Tristan Doussineau, Michel Julien, Barbara Giroud, et al.. Identification of Molecular Fragments in Equilibrium with Polysiloxane Ultrasmall Nanoparticles. Nanomaterials, 2022, 12 (5), pp.738. ⟨10.3390/nano12050738⟩. ⟨hal-03593216⟩
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- Laure Wiest, Barbara Giroud, Maëva Fieu, Azziz Assoumani, François Lestremau, et al.. Ultrasound-assisted sample preparation for simultaneous extraction of anionic, cationic and non-ionic surfactants in sediment. Talanta, 2022, pp.123220. ⟨10.1016/j.talanta.2022.123220⟩. ⟨hal-03520460⟩
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- Corentin Mit, Anne Bado-Nilles, Gaëlle Daniele, Barbara Giroud, Emmanuelle Vulliet, et al.. The toxicokinetics of bisphenol A and its metabolites in fish elucidated by a PBTK model. Aquatic Toxicology, 2022, 247, pp.106174. ⟨10.1016/j.aquatox.2022.106174⟩. ⟨hal-03702730⟩
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2021
Journal articles
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- Laure Wiest, Antoine Gosset, Aurélie Fildier, Christine Libert, Matthieu Hervé, et al.. Occurrence and removal of emerging pollutants in urban sewage treatment plants using LC-QToF-MS suspect screening and quantification. Science of the Total Environment, 2021, 774, pp.145779. ⟨10.1016/j.scitotenv.2021.145779⟩. ⟨hal-03162034⟩
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- Laure Wiest, Barbara Giroud, Azziz Assoumani, François Lestremau, Emmanuelle Vulliet. A multi-family offline SPE LC-MS/MS analytical method for anionic, cationic and non-ionic surfactants quantification in surface water. Talanta, 2021, 232, pp.122441. ⟨10.1016/j.talanta.2021.122441⟩. ⟨hal-03209496⟩
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- Barbara Giroud, Audrey Buleté, Loïc Spinner, Julie Deverchère, Léa Payen-Gay, et al.. Quantification of the organophosphate flame retardant triphenylphosphate and its main metabolite in whole blood by liquid–liquid micro-extraction and liquid chromatography-tandem mass spectrometry. Microchemical Journal, 2021, 168, pp.106374. ⟨10.1016/j.microc.2021.106374⟩. ⟨hal-03318023⟩
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- Antoine Gosset, Laure Wiest, Aurélie Fildier, Christine Libert, Barbara Giroud, et al.. Ecotoxicological risk assessment of contaminants of emerging concern identified by “suspect screening” from urban wastewater treatment plant effluents at a territorial scale. Science of the Total Environment, 2021, 778, pp.146275. ⟨10.1016/j.scitotenv.2021.146275⟩. ⟨hal-03167988⟩
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2020
Journal articles
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- Samia Selmi-Ruby, Jesús Marín-Sáez, Aurélie Fildier, Audrey Buleté, Myriam Abdallah, et al.. In vivo characterisation of the toxicological properties of DPhP, one of the main degradation products of aryl phosphate esters. Environmental Health Perspectives, 2020, 128 (12), ⟨10.1289/EHP6826⟩. ⟨hal-03013621⟩
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2019
Journal articles
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- Barbara Giroud, Selina Bruckner, Lars Straub, Peter Neumann, Geoffrey R. Williams, et al.. Trace-level determination of two neonicotinoid insecticide residues in honey bee royal jelly using ultra-sound assisted salting-out liquid liquid extraction followed by ultra-high-performance liquid chromatography-tandem mass spectrometry. Microchemical Journal, 2019, 151, pp.104249. ⟨10.1016/j.microc.2019.104249⟩. ⟨hal-02333784⟩
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2018
Journal articles
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- Alexandre Bergé, Laure Wiest, Robert Baudot, Barbara Giroud, Emmanuelle Vulliet. Occurrence of multi-class surfactants in urban wastewater: contribution of a healthcare facility to the pollution transported into the sewerage system. Environmental Science and Pollution Research, 2018, 25 (10), pp.9219-9229. ⟨10.1007/s11356-017-0470-8⟩. ⟨hal-01682871⟩
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- Gaëlle Daniele, Barbara Giroud, Claire Jabot, Emmanuelle Vulliet. Exposure assessment of honeybees through study of hive matrices: analysis of selected pesticide residues in honeybees, beebread, and beeswax from French beehives by LC-MS/MS. Environmental Science and Pollution Research, 2018, 25 (7), pp.6145-6153. ⟨10.1007/s11356-017-9227-7⟩. ⟨hal-01574982⟩
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2016
Journal articles
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- Claire Jabot, Gaëlle Daniele, Barbara Giroud, Sylvie Tchamitchian, Luc P Belzunces, et al.. Detection and quantification of boscalid and its metabolites in honeybees. Chemosphere, 2016, 156, pp.245-251. ⟨10.1016/j.chemosphere.2016.04.135⟩. ⟨hal-01355547⟩
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- Alexandre Bergé, Barbara Giroud, Laure Wiest, Bruno Domenjoud, Adriana Gonzalez-Ospina, et al.. Development of a multiple-class analytical method based on the use of synthetic matrices for the simultaneous determination of commonly used commercial surfactants in wastewater by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 2016, 1450, pp.64-75. ⟨10.1016/j.chroma.2016.04.078⟩. ⟨hal-01356449⟩
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2015
Journal articles
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- Claire Jabot, Maeva Fieu, Barbara Giroud, Audrey Buleté, Hervé Casabianca, et al.. Trace-level determination of pyrethroid, neonicotinoid and carboxamide pesticides in beeswax using dispersive solid-phase extraction followed by ultra-high-performance liquid chromatography-tandem mass spectrometry. International Journal of Environmental Analytical Chemistry, 2015, 95 (3), pp.240-257. ⟨10.1080/03067319.2015.1016011⟩. ⟨hal-01187328⟩
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2014
Journal articles
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- Yannick Poquet, Laurent Bodin, Marc Tchamitchian, Marion Fusellier, Barbara Giroud, et al.. A pragmatic approach to assess the exposure of the honey bee (Apis mellifera) when subjected to pesticide spray. PLoS ONE, 2014, 9 (11), pp.Article Number: e113728. ⟨10.1371/journal.pone.0113728⟩. ⟨hal-01230268⟩
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2013
Journal articles
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- Barbara Giroud, Antoine Vauchez, Emmanuelle Vulliet, Laure Wiest, Audrey Buleté. Trace level determination of pyrethroid and neonicotinoid insecticides in beebread using acetonitrile-based extraction followed by analysis with ultra-high-performance liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 2013, 1316, pp.53-61. ⟨10.1016/j.chroma.2013.09.088⟩. ⟨hal-00877912⟩
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- Emmanuelle Vulliet, Barbara Giroud, Pédro Marote. Determination of testosterone and its photodegradation products in surface waters using solid-phase extraction followed by LC-MS/MS analysis. Environmental Science and Pollution Research, 2013, 20 (1), pp.117-125. ⟨10.1007/s11356-012-1041-7⟩. ⟨hal-00993064⟩
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2012
Journal articles
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- Nathalie Gineys, Barbara Giroud, Mickael Gineys, Emmanuelle Vulliet. Retention of selected steroids on a silt-loam soil.. Journal of Environmental Science and Health, Part A, 2012, 47 (13), pp.2133-2140. ⟨10.1080/10934529.2012.696021⟩. ⟨hal-00965997⟩
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- Alexandra Badiou-Bénéteau, Stephan M. Carvalho, Jean-Luc Brunet, Geraldo A. Carvalho, Audrey Buleté, et al.. Development of biomarkers of exposure to xenobiotics in the honey bee Apis mellifera: Application to the systemic insecticide thiamethoxam. Ecotoxicology and Environmental Safety, 2012, 82 (1), pp.22-31. ⟨10.1016/j.ecoenv.2012.05.005⟩. ⟨hal-00924275⟩
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2011
Journal articles
- ref_biblio
- Laure Wiest, Audrey Buleté, Barbara Giroud, Cédric Fratta, Sophie Amic, et al.. Multi-residue analysis of 80 environmental contaminants in honeys, honeybees and pollens by one extraction procedure followed by liquid and gas chromatography coupled with mass spectrometric detection. Journal of Chromatography A, 2011, 1218 (34), pp.5743-5756. ⟨10.1016/j.chroma.2011.06.079⟩. ⟨hal-00639315⟩
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