Emmanuelle VULLIET

Traces, Group Leader
ISA Deputy Director
work phone: 0437423608

Research

Development of innovative analytical methods based on both targeted and untargeted strategies using mass spectrometry to investigate the exposure of environmental ecosystems and human beings to organic micropollutants and their impact on Health.

Biography

Emmanuelle Vulliet is research scientist at the Centre National de la Recherche Scientifique, France, since 2005. After a PhD at the University Lyon 1 dealing with the fate of pesticides under UV irradiations, she completed a post-doc in the Department of Physical Chemistry and Chemical Engineering of the University of A Coruña, Spain) and a Lecturer in the Laboratory of Biomolecules and Environment (University of Perpignan). She joined the Institute of Analytical Sciences (ISA) in 2005. She leads the research team TRACES of ISA and animates the transversal theme “Environment” of the Institute. She has been involved in the supervision of 9 PhD and 13 master students. She has coordinated several national projects funded by CNRS, ADEME, INSERM, FEAGA; published 71 papers in SCI journals and 3 book chapters.

Keywords

micro-pollutants; traces; metabolites, transformation products; LC-MS/MS; LC-HRMS; sample preparation; environment, exposome

Publications

Publications HAL de Emmanuelle,Vulliet

2018

Journal articles

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Alexandre Bergé, Audrey Buleté, Aurélie Fildier, R. Mailler, Johnny Gasperi, et al.. Non-target strategies by HRMS to evaluate fluidized micro-grain activated carbon as a tertiary treatment of wastewater. Chemosphere, Elsevier, 2018, 213, pp.587-595. 〈10.1016/j.chemosphere.2018.09.101〉. 〈hal-01879163〉
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Martin Sordet, Audrey Bulete, Emmanuelle Vulliet. A rapid and easy method based on hydrophilic interaction chromatography coupled with tandem mass spectrometry (HILIC-MS/MS/MS) to quantify iodinated X-ray contrast in wastewaters. Talanta, Elsevier, 2018, 190, pp.480-486. 〈10.1016/j.talanta.2018.08.006〉. 〈hal-01900226〉
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Asma Ennigrou, Hervé Casabianca, Emmanuelle Vulliet, Belgacem Hanchi, Karim Hosni. Assessing the fatty acid, essential oil composition, their radical scavenging and antibacterial activities of Schinus terebinthifolius Raddi leaves and twigs. Journal of Food Science and Technology-Mysore, 2018, pp.1582-1590. 〈10.1007/s13197-018-3049-6〉. 〈hal-01770928〉
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Alexandra Berlioz-Barbier, Audrey Buleté, Aurélie Fildier, Jeanne Garric, Emmanuelle Vulliet. Non-targeted investigation of benthic invertebrates ( Chironomus riparius ) exposed to wastewater treatment plant effluents using nanoliquid chromatography coupled to high-resolution mass spectrometry. Chemosphere, Elsevier, 2018, 196, pp.347-353. 〈10.1016/j.chemosphere.2018.01.001〉. 〈hal-01744706〉
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Laure Wiest, Teofana Chonova, Alexandre Bergé, Robert Baudot, Frédérique Bessueille-Barbier, et al.. Two-year survey of specific hospital wastewater treatment and its impact on pharmaceutical discharges. Environmental Science and Pollution Research, Springer Verlag, 2018, 25 (10), pp.9207-9218. 〈10.1007/s11356-017-9662-5〉. 〈hal-01569749〉
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Hélène Arambourou, Inmaculada Fuertes, Emmanuelle Vulliet, Gaëlle Danièle, Patrice Noury, et al.. Fenoxycarb exposure disrupted the reproductive success of the amphipod Gammarus fossarum with limited effects on the lipid profile. PLoS ONE, Public Library of Science, 2018, 13 (4), pp.Article number e0196461. 〈10.1371/journal.pone.0196461〉. 〈hal-01803483〉
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Gaëlle Daniele, Barbara Giroud, Claire Jabot, Emmanuelle Vulliet. Exposure assessment of honeybees through study of hive matrices: analysis of selected pesticide residues in honeybees, beebread, and beeswax from French beehives by LC-MS/MS. Environmental Science and Pollution Research, Springer Verlag, 2018, pp.on line. 〈10.1007/s11356-017-9227-7〉. 〈hal-01574982〉
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Agnèta Kiss, Alexandre Bergé, Bruno Domenjoud, Adriana Gonzalez-Ospina, Emmanuelle Vulliet. Chemometric and high-resolution mass spectrometry tools for the characterization and comparison of raw and treated wastewater samples of a pilot plant on the SIPIBEL site. Environmental Science and Pollution Research, Springer Verlag, 2018, 25 (10), pp.9230-9242. 〈10.1007/s11356-017-0748-x〉. 〈hal-01682862〉
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Gabrielle Magniez, Alban Franco, , Damien Rioult, Isabelle Bonnard, et al.. Determination of a new index of sexual maturity (ISM) in zebra mussel using flow cytometry: interest in ecotoxicology. Environmental Science and Pollution Research, Springer Verlag, 2018, 25 (12), pp.11252-11263. 〈10.1007/s11356-017-9256-2〉. 〈hal-01574989〉
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Alexandre Bergé, Laure Wiest, Robert Baudot, Barbara Giroud, Emmanuelle Vulliet. Occurrence of multi-class surfactants in urban wastewater: contribution of a healthcare facility to the pollution transported into the sewerage system. Environmental Science and Pollution Research, Springer Verlag, 2018, 25 (10), pp.9219-9229. 〈10.1007/s11356-017-0470-8〉. 〈hal-01682871〉
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Adriana Gonzalez-Ospina, Bruno Domenjoud, Emmanuelle Vulliet, Sylvie Bony, Sylvie Baig. Oxydation biologique et chimique à l’ozone des micropolluants émergents en station d’épuration . Environnement Risques & Santé, John Libbey Eurotext, 2018, 17 (2), pp.75-83. 〈10.1684/ers.2017.1097〉. 〈hal-01803518〉
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Adriana Wigh, Selim Ait-Aissa, Nicolas Creusot, Hugo Terrisse, Marie-Laure Delignette-Muller, et al.. Assessment of Ozone or Not-Treated Wastewater Ecotoxicity Using Mechanism-Based and Zebrafish Embryo Bioassays. Journal of Environmental Protection, 2018, 09 (04), pp.325 - 346. 〈10.4236/jep.2018.94022〉. 〈hal-01808084〉
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https://hal-univ-lyon1.archives-ouvertes.fr/hal-01808084/file/2018_Bony_J_Environ_Protect.pdf BibTex
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Charlène Pouech, Laure Wiest, Florent Lafay, Didier Léonard, Cécile Cren-Olive, et al.. Méthodes analytiques pour l'étude de la migration des additifs des conditionnements plastiques pour des applications pharmaceutiques. STP PHARMA PRATIQUES : TECHNIQUES REGLEMENTATION, 2018, 28 (3&4), pp.155-165. 〈hal-01915920〉
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2017

Journal articles

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Hélène Arambourou, Arnaud Chaumot, Emmanuelle Vulliet, Gaëlle Daniele, Nicolas Delorme, et al.. Phenotypic defects in newborn Gammarus fossarum (Amphipoda) following embryonic exposure to fenoxycarb. Ecotoxicology and Environmental Safety, Elsevier, 2017, 144, pp.193-199. 〈10.1016/j.ecoenv.2017.06.017〉. 〈hal-01574975〉
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Philippine Granger Joly de Boissel, Patrice Gonzalez, Audrey Buleté, Guillemine Daffe, Christelle Clérandeau, et al.. An innovative and integrative assay for toxicity testing using individual fish embryos. Application to oxazepam . Chemosphere, Elsevier, 2017, 181, pp.468-477. 〈10.1016/j.chemosphere.2017.04.067〉. 〈hal-01544714〉
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Maria Jesus Garcia-Galan, Martin Sordet, Audrey Buleté, Jeanne Garric, Emmanuelle Vulliet. Evaluation of the influence of surfactants in the bioaccumulation kinetics of sulfamethoxazole and oxazepam in benthic invertebrates . Science of the Total Environment, Elsevier, 2017, 592, pp.554-564. 〈10.1016/j.scitotenv.2017.03.085〉. 〈hal-01524532〉
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Gaëlle Daniele, Maëva Fieu, Sandrine Joachim, Anne Bado-Nilles, Rémy Beaudouin, et al.. Determination of carbamazepine and 12 degradation products in various compartments of an outdoor aquatic mesocosm by reliable analytical methods based on liquid chromatography-tandem mass spectrometry. Environmental Science and Pollution Research, Springer Verlag, 2017, 24 (20), pp.16893-16904. 〈10.1007/s11356-017-9297-6〉. 〈hal-01569395〉
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Aurélie Cortéjade, Audrey Buleté, Laura Prouteau, Saber Chatti, Cécile Cren, et al.. Development and optimisation of home-made stir bar sorptive extraction for analysis of plastic additives: application in human urine. Analytical Methods, Royal Society of Chemistry, 2017, 9 (23), pp.3549-3560. 〈10.1039/C7AY00696A〉. 〈hal-01546660〉
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Romain Mailler, Johnny Gasperi, Emmanuelle Vulliet, Audrey Buleté, Sam Azimi, et al.. Evaluation de l’empreinte des rejets de STEP de l’agglomération parisienne en résidus pharmaceutiques et autres polluants émergents. Revue L'Eau, L'Industrie, Les Nuisances, Johanet, 2017, pp.90-96. 〈hal-01509480〉
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Alexandre Bergé, Audrey Buleté, Aurélie Fildier, Emmanuelle Vulliet. High-Resolution Mass Spectrometry as a Tool To Evaluate the Sample Preparation of Sludge. Analytical Chemistry, American Chemical Society, 2017, 89 (18), pp.9685-9694. 〈10.1021/acs.analchem.7b01081〉. 〈hal-01583333〉
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Adriana Wigh, Olivier Geffard, Khedidja Abbaci, Adeline Francois, Patrice Noury, et al.. Gammarus fossarum as a sensitive tool to reveal residual toxicity of treated wastewater effluents. Science of the Total Environment, Elsevier, 2017, 584, pp.1012 - 1021. 〈10.1016/j.scitotenv.2017.01.154〉. 〈hal-01539979〉
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2016

Journal articles

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Claire Jabot, Gaëlle Daniele, Barbara Giroud, Sylvie Tchamitchian, Luc P Belzunces, et al.. Detection and quantification of boscalid and its metabolites in honeybees. Chemosphere, Elsevier, 2016, 156, pp.245-251. 〈10.1016/j.chemosphere.2016.04.135〉. 〈hal-01355547〉
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Gaëlle Daniele, Maéva Fieu, Sandrine Joachim, Alice James-Casas, Sandrine Andres, et al.. Development of a multi-residue analysis of diclofenac and some transformation products in bivalves using QuEChERS extraction and liquid chromatography-tandem mass spectrometry. Application to samples from mesocosm studies . Talanta, Elsevier, 2016, 155, pp.1-7. 〈10.1016/j.talanta.2016.04.016〉. 〈hal-01355557〉
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Martin Sordet, Alexandra Berlioz-Barbier, Audrey Buleté, Jeanne Garric, Emmanuelle Vulliet. Quantification of of emerging micropollutants in an amphipod crustacean by nanoliquid chromatography coupled to mass spectrometry using multiple reaction monitoring cubed mode . Journal of Chromatography A, Elsevier, 2016, 1456, pp.217-225. 〈10.1016/j.chroma.2016.06.022〉. 〈hal-01355585〉
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Laure Wiest, Robert Baudot, Emmanuelle Vulliet. Impact des rejets de médicaments sur le milieu récepteur : résultats des projets Sipibel et Irmise. Techniques Sciences Méthodes , ASTEE/EDP Sciences, 2016, pp.12-21. 〈10.1051/tsm/201606012 〉. 〈hal-01355563〉
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Adriana Gonzalez-Ospina, Bruno Domenjoud, Emmanuelle Vulliet, Agneta Kiss, Alexandre Bergé, et al.. Élimination des composés pharmaceutiques en station d’épuration par traitements biologiques et ozonation tertiaire. Techniques Sciences Méthodes , ASTEE/EDP Sciences, 2016, pp.45-58. 〈10.1051/tsm/201606045 〉. 〈hal-01355571〉
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Gaëlle Daniele, Maéva Fieu, Sandrine Joachim, Anne Bado-Nilles, Patrick Baudoin, et al.. Rapid analysis of diclofenac and some of its transformation products in the three-spined stickleback, Gasterosteus aculeatus, by liquid chromatography-tandem mass spectrometry. Analytical and Bioanalytical Chemistry, Springer Verlag, 2016, 408 (16), pp.4435-4444. 〈10.1007/s00216-016-9541-9〉. 〈hal-01356411〉
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Alexandre Bergé, Barbara Giroud, Laure Wiest, Bruno Domenjoud, Adriana Gonzalez-Ospina, et al.. Development of a multiple-class analytical method based on the use of synthetic matrices for the simultaneous determination of commonly used commercial surfactants in wastewater by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, Elsevier, 2016, 1450, pp.64-75. 〈10.1016/j.chroma.2016.04.078〉. 〈hal-01356449〉
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Yves Perrodin, Christine Bazin, Frédéric Orias, Adriana Wigh, Thérèse Bastide, et al.. A posteriori assessment of ecotoxicological risks linked to building a hospital. Chemosphere, Elsevier, 2016, 144, pp.440-445. 〈10.1016/j.chemosphere.2015.08.075〉. 〈hal-01356431〉
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Laure Wiest, Emmanuelle Vulliet. Analyse multi-résidus de pesticides dans le miel : enjeux et défis analytiques. Annales des falsifications, de l'expertise chimique et toxicologique, Société des experts-chimistes de France, 2016, 985, pp.17-27. 〈hal-01574998〉
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2015

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Mikaël Tournier, Charlène Pouech, Nadia Quignot, Florent Lafay, Laure Wiest, et al.. Determination of endocrine disruptors and endogenic androgens and estrogens in rat serum by high-performance liquid chromatography–tandem mass spectrometry. Steroids, Elsevier, 2015, 104, pp.252-262. 〈10.1016/j.steroids.2015.10.011〉. 〈hal-01241662〉
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Charlène Pouech, Agnèta Kiss, Florent Lafay, Didier Léonard, Laure Wiest, et al.. Human exposure assessment to a large set of polymer additives through the analysis of urine by solid phase extraction followed by ultra high performance liquid chromatography coupled to tandem mass spectrometry. Journal of Chromatography A, Elsevier, 2015, 1423, pp.111-123. 〈10.1016/j.chroma.2015.10.091〉. 〈hal-01241519〉
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Alexandre Bergé, Emmanuelle Vulliet. Development of a method for the analysis of hormones and pharmaceuticals in earthworms by quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction followed by liquid chromatography-tandem mass spectrometry (LC-MS/MS). Analytical and Bioanalytical Chemistry, Springer Verlag, 2015, 407 (26), pp.7995-8008. 〈10.1007/s00216-015-8972-z〉. 〈hal-01229268〉
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Claire Jabot, Maeva Fieu, Barbara Giroud, Audrey Buleté, Hervé Casabianca, et al.. Trace-level determination of pyrethroid, neonicotinoid and carboxamide pesticides in beeswax using dispersive solid-phase extraction followed by ultra-high-performance liquid chromatography-tandem mass spectrometry. International Journal of Environmental Analytical Chemistry, Taylor & Francis, 2015, 95 (3), pp.240-257. 〈10.1080/03067319.2015.1016011〉. 〈hal-01187328〉
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Julien Camilleri, Robert Baudot, Laure Wiest, Emmanuelle Vulliet, Cécile Cren-Olivé, et al.. Multiresidue fully automated online SPE-HPLC-MS/MS method for the quantification of endocrine-disrupting and pharmaceutical compounds at trace level in surface water. International Journal of Environmental Analytical Chemistry, Taylor & Francis, 2015, 95 (1), pp.67-81. 〈10.1080/03067319.2014.983494〉. 〈hal-01119523〉
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Marie-Virginie Salvia, Maeva Fieu, Emmanuelle Vulliet. Determination of tetracycline and fluoroquinolone antibiotics at trace levels in sludge and soil. Applied and Environmental Soil Science, Hindawi Publishing Corporation, 2015, 2015, pp.article ID 435741. 〈10.1155/2015/435741〉. 〈hal-01356467〉
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Julien Camilleri, Emmanuelle Vulliet. Determination of steroid hormones in sediments based on quick, easy, cheap, effective, rugged, and safe (modified-QuEChERS) extraction followed by liquid chromatography-tandem mass spectrometry (LC-MS/MS). Analytical Methods, Royal Society of Chemistry, 2015, 7 (22), pp.9577-9586. 〈10.1039/c5ay01972a〉. 〈hal-01241666〉
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2014

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Alexandra Berlioz-Barbier, Audrey Buleté, Juliette Fabure, Jeanne Garric, Cécile Cren-Olivé, et al.. Multi-residue analysis of emerging pollutants in benthic invertebrates by modified micro-quick-easy-cheap-efficient-rugged-safe extraction and nanoliquid chromatography-nanospray-tandem mass spectrometry analysis. Journal of Chromatography A, Elsevier, 2014, 1367, pp.16-32. 〈10.1016/j.chroma.2014.09.044〉. 〈hal-01230302〉
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Emmanuelle Vulliet, Alexandra Berlioz-Barbier, Florent Lafay, Robert Baudot, Laure Wiest, et al.. A national reconnaissance for selected organic micropollutants in sediments on French territory. Environmental Science and Pollution Research, Springer Verlag, 2014, 21, 19, pp.11370-11379. 〈10.1007/s11356-014-3089-z〉. 〈hal-01230435〉
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Marie-Virginie Salvia, Cécile Cren-Olivé, Laure Wiest, Robert Baudot, Emmanuelle Vulliet. Comparison of Two Analytical Methods for the Determination of Traces of Veterinary Antibiotics and Steroid Hormones in Soil Based on Pressurised Liquid Extraction (PLE) and Quick, Easy, Cheap, Effective, Rugged, Safe (Modified-Quechers) Extraction. Pharmaceutica Analytica Acta, OMICS publishing group, 2014, 5 (9), pp.1000315. 〈10.4172/2153-2435.1000315〉. 〈hal-01100640〉
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Marie-Virginie Salvia, Julie Experton, Claire Geandel, Cécile Cren-Olivé, Emmanuelle Vulliet. Fate of pharmaceutical compounds and steroid hormones in soil: study of transfer and degradation in soil columns.. Environmental Science and Pollution Research, Springer Verlag, 2014, 21 (17), pp.10525-10535. 〈10.1007/s11356-014-3038-x〉. 〈hal-01070854〉
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Emmanuelle Vulliet, Mikaël Tournier, Antoine Vauchez, Laure Wiest, Robert Baudot, et al.. Survey regarding the occurrence of selected organic micropollutants in the groundwaters of overseas departments. Environmental Science and Pollution Research, Springer Verlag, 2014, 21 (12), pp.7512-7521. 〈10.1007/s11356-014-2619-z〉. 〈hal-01071649〉
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Raphael Santos, Mélissa Palos-Ladeiro, Aurélien Besnard, Emmanuelle Vulliet, Jean-Marc Porcher, et al.. Kinetic response of a genotoxicity biomarker in the three-spined stickleback and implication for environmental monitoring. Ecotoxicology and Environmental Safety, Elsevier, 2014, 102, pp.6-11. 〈10.1016/j.ecoenv.2014.01.006〉. 〈hal-00942152〉
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Alexandra Berlioz-Barbier, Antoine Vauchez, Laure Wiest, Robert Baudot, Emmanuelle Vulliet, et al.. Multi-residue analysis of emerging pollutants in sediment using QuEChERS-based extraction followed by LC-MS/MS analysis.. Analytical and Bioanalytical Chemistry, Springer Verlag, 2014, 406 (4), pp.1259-1266. 〈10.1007/s00216-013-7450-8〉. 〈hal-00955924〉
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2013

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Barbara Giroud, Antoine Vauchez, Emmanuelle Vulliet, Laure Wiest, Audrey Buleté. Trace level determination of pyrethroid and neonicotinoid insecticides in beebread using acetonitrile-based extraction followed by analysis with ultra-high-performance liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, Elsevier, 2013, 1316, pp.53-61. 〈10.1016/j.chroma.2013.09.088〉. 〈hal-00877912〉
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Marie-Virginie Salvia, Cécile Cren-Olivé, Emmanuelle Vulliet. Statistical evaluation of the influence of soil properties on recoveries and matrix effects during the analysis of pharmaceutical compounds and steroids by quick, easy, cheap, effective, rugged and safe extraction followed by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, Elsevier, 2013, 1315, pp.53-60. 〈10.1016/j.chroma.2013.09.056〉. 〈hal-00877918〉
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R. Santos, M. Palos-Ladeiro, A. Besnard, J. Reggio, Emmanuelle Vulliet, et al.. Parental exposure to methyl methane sulfonate of three-spined stickleback: contribution of DNA damage in male and female germ cells to further development impairment in progeny. Ecotoxicology, Springer Verlag, 2013, 22 (5), pp.815-824. 〈10.1007/s10646-013-1088-3〉. 〈hal-00860498〉
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Mélanie Villeret, Sabrina Jolly, Laure Wiest, Emmanuelle Vulliet, Anne Bado-Nilles, et al.. A potential biomarker of androgen exposure in European bullhead (Cottus sp.) kidney. Fish Physiology and Biochemistry, Springer Verlag, 2013, 39 (3), pp.573-580. 〈10.1007/s10695-012-9720-3〉. 〈hal-00860752〉
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https://hal.archives-ouvertes.fr/hal-00860752/file/2012-338_post-print.pdf BibTex
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William Peysson, Emmanuelle Vulliet. Determination of 136 pharmaceuticals and hormones in sewage sludge using quick, easy, cheap, effective, rugged and safe extraction followed by analysis with liquid chromatography-time-of-flight-mass spectrometry. Journal of Chromatography A, Elsevier, 2013, 1290, pp.46-61. 〈10.1016/j.chroma.2013.03.057〉. 〈hal-00825023〉
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Emmanuelle Vulliet, Barbara Giroud, Pédro Marote. Determination of testosterone and its photodegradation products in surface waters using solid-phase extraction followed by LC-MS/MS analysis. Environmental Science and Pollution Research, Springer Verlag, 2013, 20 (1), pp.117-125. 〈10.1007/s11356-012-1041-7〉. 〈hal-00993064〉
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2012

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Marie-Virginie Salvia, Emmanuelle Vulliet, Laure Wiest, Robert Baudot, Cécile Cren-Olivé. Development of a multi-residue method using acetonitrile-based extraction followed by liquid chromatography-tandem mass spectrometry for the analysis of steroids and veterinary and human drugs at trace levels in soil. Journal of Chromatography A, Elsevier, 2012, 1245, pp.122-133. 〈10.1016/j.chroma.2012.05.034〉. 〈hal-00705807〉
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Nathalie Gineys, Barbara Giroud, Mickael Gineys, Emmanuelle Vulliet. Retention of selected steroids on a silt-loam soil.. Journal of Environmental Science and Health, Part A, Taylor & Francis, 2012, 47 (13), pp.2133-2140. 〈10.1080/10934529.2012.696021〉. 〈hal-00965997〉
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2011

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Karim Hosni, Marwa Jemli, Salma Dziri, Yacine M'Rabet, Asma Ennigrou, et al.. Changes in phytochemical, antimicrobial and free radical scavenging activities of the Peruvian pepper tree (Schinus molle L.) as influenced by fruit maturation. Industrial Crops and Products, Elsevier, 2011, 34 (3), pp.1622-1628. 〈10.1016/j.indcrop.2011.06.004〉. 〈hal-00616337〉
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Camille Pasquet, Emmanuelle Vulliet. Utilisation of an enzyme-linked immunosorbent assay (ELISA) for determination of alkylphenols in various environmental matrices. Comparison with LC-MS/MS method. Talanta, Elsevier, 2011, 85 (5), pp.2492-2497. 〈10.1016/j.talanta.2011.07.102〉. 〈hal-00639311〉
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Emmanuelle Vulliet, Cécile Cren-Olivé, Marie-Florence Grenier-Loustalot. Occurrence of pharmaceuticals and hormones in drinking water treated from surface waters. Environmental Chemistry Letters, Springer Verlag, 2011, 9 (1), pp.103-114. 〈10.1007/s10311-009-0253-7〉. 〈hal-00509280〉
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Emmanuelle Vulliet, Cécile Cren-Olivé. Screening of pharmaceuticals and hormones at regional scale, in surface and groundwaters intended to human consumption. Environmental Pollution, Elsevier, 2011, 159 (10), pp.2929-2934. 〈10.1016/j.envpol.2011.04.033〉. 〈hal-00616322〉
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